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http://cimav.repositorioinstitucional.mx/jspui/handle/1004/1142| New Synthesis Method to Obtain Pd Nano-Crystals | |
| MARTHA TERESITA OCHOA LARA JOSE JESUS CARLOS QUINTANAR SIERRA | |
| Acceso Abierto | |
| Sin Derechos Reservados | |
| palladium nano-crystal TGA HRSEM | |
| We report a new synthesis method to obtain palladium nano-crystals by sol-gel polymerized with acrylamide. From thermogravimetric analysis (TGA) studies, we found PdO and Pd compounds in the xerogel sample, at 550 ºC, and over 900 ºC we detected only metallic Pd. These results were corroborated by powder X-Ray Diffraction (XRD), High Resolution Scanning Electron Microscopy (HRSEM), and Transmission Electron Microscopy (TEM). XRD studies exhibit the lines from the tetragonal structure (PDF 41-1107) of PdO compound and from the cubic structure (PDF 46-1043) of Pd metallic. HRSEM micrographs show morphologies from the sample very sensitive to heat treatment. Finally, TEM images show crystals of ~8 nm in diameter. | |
| 2011 | |
| Artículo | |
| Inglés | |
| OTRAS | |
| Versión revisada | |
| submittedVersion - Versión revisada | |
| Aparece en las colecciones: | Artículos |
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| New Synthesis Method to Obtain Pd Nano-Crystals PDF 2011.pdf | 547.58 kB | Adobe PDF | Visualizar/Abrir |