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Growth and microstructural study of CuO covered ZnO nanorods
JOSE FRANCISCO POLA ALBORES
WILBER ANTUNEZ FLORES
PATRICIA AMEZAGA MADRID
EDNA IRIS RIOS VALDOVINOS
MIGUEL ANGEL VALENZUELA ZAPATA
FRANCISCO PARAGUAY DELGADO
MARIO MIKI YOSHIDA
Acceso Abierto
Sin Derechos Reservados
Rietveld Refinement
CuO
A feasiblemethod to synthesize CuO covered ZnO nanorods was realized. Firstly, ZnO nanorods were grown by wet-chemical route at 90 °C onto borosilicate glass substrates. Subsequently, the CuO covered ZnO matrix was obtained by Aerosol-Assisted Chemical Vapor Deposition at different temperatures (300, 400, 500 and 600°C). The CuO–ZnO nanocrystals were microstructurally characterized by electron microscopy and Rietveld refinement. Results showed a CuO formed nanocrystals but also an amorphous fraction of CuO which increases with the synthesis temperature. Additionally, it was evident the presence of secondary copper-oxide phase (paramelaconite), which also has grown over the ZnO nanorod surface.
2012
Artículo
Inglés
OTRAS
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