Por favor, use este identificador para citar o enlazar este ítem: http://cimav.repositorioinstitucional.mx/jspui/handle/1004/1011
Study of iron oxides obtained by decomposition of an organic precursor
JOSE ANDRES MATUTES AQUINO
PERLA ELVIA GARCIA CASILLAS
OSCAR EDUARDO AYALA VALENZUELA
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Iron oxides
Iron oxide powders were obtained by the isothermal decomposition of ferric citrate in an oxygen atmosphere at different temperatures. Throughout the experiments, the product of decomposition was a mixture of maghemite (ϒ-Fe2O3) and hematite (α-Fe2O3. with different relative proportions and particle size distributions. After TGA and DTA measurements, a decomposition temperature of 300°C was chosen, and a maximum specific saturation magnetization of about 40 emurg was obtained. Most of the product particles were less than 1 μm in size, including a superparamagnetic fraction, as evidenced by Mössbauer spectroscopy.
1999
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