Por favor, use este identificador para citar o enlazar este ítem:
http://cimav.repositorioinstitucional.mx/jspui/handle/1004/1828| Microstructural, chemical and textural characterization of ZnO nanorods synthesized by aerosol assisted chemical vapor deposition | |
| ANGELICA SAENZ TREVIZO PATRICIA AMEZAGA MADRID LUIS EDMUNDO FUENTES COBAS PEDRO PIZA RUIZ WILBER ANTUNEZ FLORES CARLOS ELIAS ORNELAS GUTIERREZ SILVIA ADRIANA PEREZ GARCIA MARIO MIKI YOSHIDA | |
| Acceso Abierto | |
| Sin Derechos Reservados | |
| ZnO nanorods 2D X-ray diffraction | |
| ZnO nanorods were synthesized by aerosol assisted chemical vapor deposition onto TiO2 covered borosilicate glass substrates. Deposition parameters were optimized and kept constant. Solely the effect of different nozzle velocities on the growth of ZnO nanorods was evaluated in order to develop a dense and uniform structure. The crystalline structure was characterized by conventional X-ray diffraction in grazing incidence and Bragg–Brentano configurations. In addition, two-dimensional grazing incidence synchrotron radiation diffraction was employed to determine the preferred growth direction of the nanorods. Morphology and growth characteristics analyzed by electron microscopy were correlated with diffraction outcomes. Chemical composition was established by X-ray photoelectron spectroscopy. X-ray diffraction results and X-ray photoelectron spectroscopy showed the presence of wurtzite ZnO and anatase TiO2 phases. Morphological changes noticed when the deposition velocity was lowered to the minimum, indicated the formation of relatively vertically oriented nanorods evenly distributed onto the TiO2 buffer film. By coupling two-dimensional X-ray diffraction and computational modeling with ANAELU it was proved that a successful texture determination was achieved and confirmed by scanning electron microscopy analysis. Texture analysis led to the conclusion of a preferred growth direction in [001] having a distribution width Ω=20° ± 2°. | |
| 2014 | |
| Memoria de congreso | |
| Inglés | |
| OTRAS | |
| Versión revisada | |
| submittedVersion - Versión revisada | |
| Aparece en las colecciones: | Artículos |
Cargar archivos:
| Fichero | Tamaño | Formato | |
|---|---|---|---|
| Microstructural, chemical and textural characterization of ZnO nanorods synhtesized by aerosol assisted chemical vapor deposition PDF.pdf | 1.24 MB | Adobe PDF | Visualizar/Abrir |