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Temperature effect on dipolar and exchange interactions for SmCo5+lFe65Co35 nanocomposite powders
LAURA PATRICIA MUÑOZ ORTEGA
JOSE TRINIDAD ELIZALDE GALINDO
JOSE RURIK FARIAS MANCILLA
JOSE ANDRES MATUTES AQUINO
Acceso Abierto
Sin Derechos Reservados
Nanocomposite powders
DC magnetization measurements were used to determine the temperature dependencies of the magnetic properties for (90%wt)SmCo5+(10%wt)Fe65Co35 nanocomposite powders synthesized by mechanical milling and subsequent annealing. The annealing conditions were T equal to 1073K and time, t, equal to 1.5, 3.0, 4.5, 6.0 min. Maximum magnetization decreased upon cooling in temperature range from 290 to 10 K. Coercivity increased its value to a maximum at the lowest temperature. On the other hand, hysteresis loops collected at low temperatures showed a “knee” in the second quadrant of the demagnetization curve, which suggests that dipolar interactions are becoming stronger than intergrain exchange coupling as temperature is lowered. This low temperature reduction of exchange interactions is confirmed by the temperature dependence of the exchange coupled volume ratio, R. Finally, the temperature effect on magnetic properties is explained on the basis of anisotropy enhancement and reduction of thermal fluctuations as temperature decreases.
2012
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