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http://cimav.repositorioinstitucional.mx/jspui/handle/1004/2232| Microstructural Study of ZnO Nanostructures by Rietveld Analysis | |
| JOSE FRANCISCO POLA ALBORES FRANCISCO PARAGUAY DELGADO WILBER ANTUNEZ FLORES PATRICIA AMEZAGA MADRID MARIO MIKI YOSHIDA | |
| Acceso Abierto | |
| Sin Derechos Reservados | |
| ZnO | |
| ZnO nanorods were synthesized by induced seeds by chemical bath deposition using hexamethylenetetramine (HMT) as a precipitant agent and zinc nitrate (ZN) as Zn2+ source at 90◦C. The influence of reactants ratio was studied from2 to 0.25 ZN/HMT molar. The results obtained by scanning electron microscopy confirm that the diameter of nanorods was affected directly by the concentration of both zinc and OH− sources. Nanotubes (hollow nanorods) were obtained with high HMT concentrations and were turning over nanorods as HMT concentration decreased. Microstructural information was obtained by Rietveld refinement of grazing incidence X-ray diffraction data. These results evidence low-textured materials with oriented volumes less than 18% coming from (101) planes in Bragg condition. | |
| 2011 | |
| Artículo | |
| Inglés | |
| OTRAS | |
| Versión revisada | |
| submittedVersion - Versión revisada | |
| Aparece en las colecciones: | Artículos |
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| Microstructural Study of ZnO Nanostructures by PDF 2011.pdf | 796.01 kB | Adobe PDF | Visualizar/Abrir |